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Laboratory scale supercritical extraction systems


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Summary

TharSFC offer a range of SFE srigs for laboratory scale work. These simple to use systems off er the user the following key benefits:

  • Modular system: this makes it flexible and can be easily modified
  • Computer controlled: all flow,temperature and pressure settings are controlled via a user friendly software
  • Rated to 690bar ( 10,000PSI)
  • Available from 100ml to 5L
  • Turn key package, ready to use after short insallation
  • All key components made by Thar SFC

Design Features

The modualar design of the rigs

The 6100 Calorimeter is intended for the user who wants a modern calorimeter with the convenient automatic features provided in the 6200 Calorimeter and whose precision requirements can be met with a static system without isoperibol control. Or, for users whose work load is small or intermittent, making it preferable to purchase a lower cost model. To meet these criteria, the temperature controlled water jacket and its accessories have been removed from the 6200 Calorimeter and replaced in the 6100 with a static air jacket around the bucket chamber, comparable to the arrangement used in the 1341 Plain Calorimeter. This eliminates all water and water connections, resulting in a significant saving in cost.

All sensors and controls in the 6100 Calorimeter are built into a single, compact cabinet to provide a self-contained operating unit consisting of:

  • An 1108 oxygen bomb with an oval bucket which fits into the insulating water jacket.
  • A built-in semi-automatic system for charging the bomb with oxygen.
  • A high precision electronic thermometer.
  • A bright, color, touch screen display for data entry and operation control.
  • Special communication ports for printer, computer and network (LAN) connections.
  • Removable compact flash memory card slot for simple program updates and test report archiving.

Good Repeatability

To obtain the best precision with an uncontrolled jacket, the 6100 Calorimeter has a temperature monitoring capability built into the jacket. This allows the calorimeter to measure the actual jacket temperature and apply the appropriate heat leak corrections in real time. While not equal to an isolating water jacket, the 6100 method offers a significant improvement over the traditional static jacket and makes it possible to obtain reasonable precision without the long pre- and post-periods normally required for static jacket calorimetry. It also makes it possible to use the Parr Dynamic Method for rapid testing.

As with all static jacket calorimeters, best results will be obtained when the calorimeter is operated in a location where it is not subject to drafts or fluctuating air temperature, preferable in a temperature-controlled room. It may require more frequent standardization if the ambient temperature changes during the day or from day to day. With these constrictions under control, standard deviations in a series of tests with a uniform sample, such as benzoic acid, should not exceed 0.2 percent. The precision obtainable will be more than adequate for most waste screening and teaching applications. .

A Self-Contained Operating Unit

The 6100 Calorimeter is a compact operating unit that uses the same 1108 oxygen bomb and oval bucket furnished with the 6200 or with the 1266 and 1356 previous models. It also has the same automatic oxygen filling system and high precision electronic thermometer used in the 6200 Calorimeter. There is a touch-panel keyboard for data entry and a color LCD display for operator prompts, status indication, data verification and report views. All steps in the test procedure are managed by a microprocessor control system programmed to operate the calorimeter in either the conventional equilibrium mode or in a faster dynamic mode. All data is handled automatically by a dedicated microcomputer.

Printed Reports

An optional 1757 Printer can be furnished with each 6100 Calorimeter to produce a permanent record of all activity within the calorimeter.


For further information and prices, please click here.

Please also visit the Parr Website for further information:

1341



Forr further information and prices on any of the above, please click here.

Please also visit the Thar Website for further information:

WWW.THARSFC.COM



Shirley House,   12 Gatley Road,   Cheadle,   Cheshire,   SK8 1PY.    T: +44 (0) 161 491 3068    E: enquiries@scimed.co.uk